Chemical Instrumentation 6614 Spring 2018

LABS

Lab#	Date run in lab	Lab title	Due date
		Lab Syllabus
		Model Lab report
1	1 Feb	Preparation of Molar and Standard Addition Cu & Ni Solutions	8 Feb
		Rubric For Lab 1
2	8 Feb	UV-VIS Analysis of an Unknown Cu(II) + Ni(II) Mixture	15 Feb
		Rubric for Lab 2
3	15 Feb	AAS Standard Analysis of an Unknown Cu(II) Ni(II) Mixture	22 Feb
		Rubric for Lab 3
4a	22 Feb	FTIR Band Analysis (Qualitative IR)	1 March
		Rubric for Lab 4a
4b	1 March	Environmental Sleuthing (Quantitative IR)	8 March
		Rubric for Lab 4b
5	8 March	IR/GC Analysis of an Unknown Mixture	22 March (post break)
		Rubric for Lab 5
6 (dry)	22 March	HPLC Dry Lab (rubric within Lab)	29 March
6		HPLC Analysis of aromatic mixture and estimation of Instrument Detection limit	Use with HPLC dry lab
		Answers to HPLC dry lab
7	29 March	Introduction to Mass Spectroscopy: Analysis of a Single Unknown Fragmentation Pattern	5 April
		Rubric for Lab 7
8	5 April	GC/MS Drug bust scenario	12 April
		Rubric for lab 8
9	13 April	Scientific Lampworking (Glass blowing exercise)	19 April (pieces due)
		Rubric-pieces pass the Mean Dave `break’ test
10a	19 April	Koehler Illumination	20 April-27 April (by appt.)
		Rubric – misaligned scope is returned to Koehler condition
10b	19 April	Chemical Microscopy	26 April
		Flow Scheme and Test Protocols for Experiment 10b
		Rubric for Lab 10b
	26 April	Final Unknown Assignment	Due day of Instrumentation final (or earlier)
	26 April & 3 May	oral instrumentation practicum-random date and instrument pick: 10-15 minutes/student	26 April & 3 May