Chemical Instrumentation 6614 Spring 2015

LABS

Lab#	Date run in lab	Lab title	Due date
		Lab Syllabus
		Model Lab report
1	5 Feb	Preparation of Molar and Standard Addition Cu & Ni Solutions	12 Feb
		Rubric For Lab 1
2	12 Feb	UV-VIS Analysis of an Unknown Cu(II) + Ni(II) Mixture	19 Feb
		Rubric for Lab 2
3	19 Feb	AAS Standard Analysis of an Unknown Cu(II) Ni(II) Mixture	26 Feb
		Rubric for Lab 3
4a	26 Feb	FTIR Band Analysis (Qualitative IR)	5 March
		Rubric for Lab 4a
4b	5 March	Environmental Sleuthing (Quantitative IR)	12 March
		Rubric for Lab 4b
5	12 March	IR/GC Analysis of an Unknown Mixture	26 March (post break)
		Rubric for Lab 5
6 (dry)	26 March	HPLC Dry Lab (rubric within Lab)	2 April
6		HPLC Analysis of aromatic mixture and estimation of Instrument Detection limit	Use with HPLC dry lab
7	2 April	Introduction to Mass Spectroscopy: Analysis of a Single Unknown Fragmentation Pattern	9 April
		Rubric for Lab 7
8	9 April	GC/MS Drug bust scenario	16 April
		Rubric for lab 8
9	16 April	Scientific Lampworking (Glass blowing exercise)	23 April (pieces due)
		Rubric-pieces pass the Mean Dave `break’ test
10a	23 April	Koehler Illumination	23 April-30 April (by apt.)
		Rubric – misaligned scope is returned to Koehler condition
10b	23 April	Chemical Microscopy	30 April
		Rubric for Lab 10b
	30 April	oral instrumentation practicum-random pick	Day of final (Answer only + oral)